Bipolarolides A–G: Ophiobolin‐Derived Sesterterpenes with Three New Carbon Skeletons from Bipolaris sp. TJ403‐B1

Angewandte Chemie International Edition
2019.0

Abstract

<jats:title>Abstract</jats:title><jats:p>Bipolarolides A–G (<jats:bold>1</jats:bold>–<jats:bold>7</jats:bold>), seven novel ophiobolin‐derived sesterterpenes with three new types of skeletons, were characterized from fungus <jats:italic>Bipolaris</jats:italic> sp. TJ403‐B1. Their structures were determined via spectroscopic analyses, X‐ray crystallography, and quantum chemical <jats:sup>13</jats:sup>C NMR and electronic circular dichroism (ECD) calculations. Compounds <jats:bold>1</jats:bold> and <jats:bold>2</jats:bold> were uniquely defined by a multicyclic caged oxapentacyclo[9.3.0.0<jats:sup>1,6</jats:sup>.0<jats:sup>5,9</jats:sup>.1<jats:sup>8,12</jats:sup>]pentadecane‐bridged system. Compounds <jats:bold>3</jats:bold> and <jats:bold>4</jats:bold> featured an unprecedented 5‐5‐5‐5‐fused core skeleton, while <jats:bold>3</jats:bold> also contained an unexpected C‐3–C‐14 oxygen bridge to construct the caged architecture. Compounds <jats:bold>5</jats:bold>–<jats:bold>7</jats:bold> form a new class of highly modified pentacyclic oxaspiro[4.4]nonane‐containing sesterterpene‐alkaloid hybrids. Their biosynthetic pathways and potential HMG‐CoA reductase inhibitory and antimicrobial activities are also discussed.

Knowledge Graph

Similar Paper

Bipolarolides A–G: Ophiobolin‐Derived Sesterterpenes with Three New Carbon Skeletons from <i>Bipolaris</i> sp. TJ403‐B1
Angewandte Chemie International Edition 2019.0
Bipolarolides A–G: Ophiobolin‐Derived Sesterterpenes with Three New Carbon Skeletons from Bipolaris sp. TJ403‐B1
Angewandte Chemie International Edition 2019.0
Bipolaricins A–I, Ophiobolin-Type Tetracyclic Sesterterpenes from a Phytopathogenic <i>Bipolaris</i> sp. Fungus
Journal of Natural Products 2019.0
3-Anhydro-6-hydroxy-ophiobolin A, a new sesterterpene inhibiting the growth of methicillin-resistant Staphylococcus aureus and inducing the cell death by apoptosis on K562, from the phytopathogenic fungus Bipolaris oryzae
Bioorganic &amp; Medicinal Chemistry Letters 2013.0
Caryophyllenes from a Fungal Culture of <i>Chrysosporium</i> <i>pilosum</i>
Journal of Natural Products 2009.0
Ophiobolin Sesterterpenoids and Farnesylated Phthalide Derivatives from the Deep Sea Cold-Seep-Derived Fungus <i>Aspergillus insuetus</i> SD-512
Journal of Natural Products 2020.0
Ophiobolin-Type Sesterterpenoids from the Mangrove Endophytic Fungus <i>Aspergillus</i> sp. ZJ-68
Journal of Natural Products 2019.0
Bipolamides A and B, triene amides isolated from the endophytic fungus Bipolaris sp. MU34
The Journal of Antibiotics 2014.0
Highly Oxygenated Caryophyllene-Type Sesquiterpenes from a Plant-Associated Fungus, <i>Pestalotiopsis hainanensis</i>, and Their Biosynthetic Gene Cluster
Journal of Natural Products 2020.0
Polyoxygenated Bipyridine, Pyrrolylpyridine, and Bipyrrole Alkaloids from <i>Speranskia tuberculata</i>
Journal of Natural Products 2000.0