<p>Gilluones A–C (<bold>1–3</bold>), three new phloroglucinol heterodimers, asterriquinones I–K (<bold>4–6</bold>), three new bis-indolylquinones, and asterriquinols G–I (<bold>7–9</bold>), three new bis-indolylbenzenoids, were isolated from the sponge-derived fungus <italic>Aspergillus</italic> sp. SCSIO 41018.</p>