Structural characterization of saturated pyrrolizidine alkaloids from Heliotropium transalpinum var. transalpinum Vell by NMR spectroscopy and theoretical calculations

Tetrahedron Letters
2009.0

Abstract

The chemical investigation of Heliotropium transalpinum var. transalpinum Vell. (Boraginaceae) led to the isolation of transalpinecine (1), a novel pyrrolizidine alkaloid, in addition to known alkaloids subulacine (1β-2β-epoxy-1α-hydroxymethyl-8α-pyrrolizidine) (2), and 1α-2α-epoxy-1β-hydroxymethyl-8α-pyrrolizidine (3). The structures of the isolated compounds were elucidated based on spectroscopic data and theoretical calculations. © 2009 Elsevier Ltd. All rights reserved.

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