Synthesis of 1-Deoxy-1-hydroxymethyl- and 1-Deoxy-1-epi-hydroxymethyl Castanospermine as New Potential Immunomodulating Agents

Journal of Medicinal Chemistry
2007.0

Abstract

Two new C-1 epimeric hydroxymethyl castanospermine congeners 2a and 2b, synthesized by stereocon trolled intramolecular double reductive amination Of D-glucose derived beta-keto ester as a key step, showed impressive immuno-potentiating property. The bioactivity was mediated through up-regulation of T-H1/T-H2 cytokine ratio. The finding suggested that immunmodulatory activity of polyhydroxylated indolizidine alkaloids can be tuned by minor structural/stereochemical alterations.

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