The volatile leaf oils of Eucalyptus cornuta Labill., E. talyuberlup D.J. Carr & S.G.M. Carr, E. newbeyi D.J. Carr & S.G.M. Carr, E. burdettiana Blakely & Steedman, E. megacornuta C.A. Gardner, E. lehmannii (Schauer) Benth., E. conferruminata D.J. Carr & S.G.M. Carr, E. bakeri Maiden, E. jutsonii Maiden, E. mannensis Boomsma subsp. mannensis, E. leptocalyx Blakely, E. scyphocalyx (F. Muell. ex Benth.) Maiden & Blakely, E. platycorys Maiden & Blakely isolated by vacuum distillation, were analysed by GC-MS. Most species contained a-pinene (1.1-46%), 1,8-cineole (0.2-86.1%), aromadendrene/terpinen-4-ol (0-9.5%) and trans-pinocarveol (0.1-13.3%) as principal leaf oil components.