The structures of telisatins A and B [2] and telitoxinone [3], three new aporphinoid alkaloids isolated from a neutral fraction of Telitoxicum peruvianum, were determined by spectral data interpretation. Telitoxicum peruvianum Moldenke (Menispermaceae) was used by the Huitoto Indians of Peru as an ingredient of curare (1). We have reported previously the alkaloids isolated from the basic fraction of this species as azafluoranthenes, oxoaporphines, and other aporphinoids (2). The presence of additional alkaloids in a neutral fraction of T. krukmii (3) led us to investigate the same fraction of T. peruvianum, which yielded telisatins A and B (both of which are reported here from a plant source for the first time), along with two oxoaporphines, lysicamine and O-methylmoschatoline, as well as telitoxinone {3}.