<jats:title>Abstract</jats:title><jats:p>Twenty‐four compounds including three flavonoids, kaempferol‐3‐<jats:italic>O</jats:italic>‐rhamnoside (<jats:bold>1</jats:bold>), quercetin‐3‐<jats:italic>O</jats:italic>‐rhamnoside (<jats:bold>2</jats:bold>), and taxifolin‐3‐<jats:italic>O</jats:italic>‐rhamnoside (<jats:bold>3</jats:bold>); three ferulates, docosanylferulate (<jats:bold>4</jats:bold>), tetracosanylferulate (<jats:bold>5</jats:bold>), and hexacosanylferulate (<jats:bold>6</jats:bold>); two cyclohex‐2‐en‐1‐ones, blumenol A (<jats:bold>7</jats:bold>), and roseoside (<jats:bold>8</jats:bold>); two sesquiterpenes, zeylanidine (<jats:bold>9</jats:bold>), and zeylanicine (<jats:bold>10</jats:bold>); four triterpenes, lupeol (<jats:bold>11</jats:bold>), lupenone (<jats:bold>12</jats:bold>), taraxerol (<jats:bold>13</jats:bold>), and taraxerone (<jats:bold>14</jats:bold>); one steroid, β‐sitosterol (<jats:bold>15</jats:bold>); one amide, <jats:italic>N‐trans</jats:italic>‐feruloylmethoxytyramine (<jats:bold>16</jats:bold>); eight alkaloids, roemerine (<jats:bold>17</jats:bold>), actinodaphnine (<jats:bold>18</jats:bold>), <jats:italic>N</jats:italic>‐methylactinodaphnine (<jats:bold>19</jats:bold>), glaucine (<jats:bold>20</jats:bold>), and oxoglaucine (<jats:bold>21</jats:bold>), boldine (<jats:bold>22</jats:bold>), corydine (<jats:bold>23</jats:bold>) and methoxyannomontine (<jats:bold>24</jats:bold>) were isolated from <jats:italic>Neolitsea parvigemma</jats:italic> and <jats:italic>N. konishii.</jats:italic> These compounds were characterized and identified by physical and spectral evidence. Among them, compounds <jats:bold>1, 2, 3, 4, 5, 6, 7, 8, 13, 14, 16, 20, 21, 23</jats:bold>, and <jats:bold>24</jats:bold>, were isolated for the first time from this genus. This finding is useful as a basis for chemotaxonomy.