<jats:title>Abstract</jats:title><jats:p>Twenty‐nine compounds including three alkaloids, live triterpenoids, five coumarins, seven benzenoids, two tannins, five flavonoids, one sugar and one nucleoside are isolated from leaves of <jats:italic>Tetradium glabrifolium</jats:italic>. Their structures are characterized on comparison of spectral data with literature values.